مشخصات پژوهش

صفحه نخست /Solid phase extraction of ...
عنوان
Solid phase extraction of acetaminophen by magnetic expanded graphite sorbentfunctionalized with glycine and its quantitative determination by gold-silver nanoparticlefunctionalized with polyethyleneimine as a colorimetric sensor
نوع پژوهش مقاله ارائه شده
کلیدواژه‌ها
Acetaminophen ، Expanded graphite ، Gold-silver nanoparticles ، Magnetic sorbent
چکیده
A solid phase extraction method using magnetic expanded graphite sorbent was proposed for theseparation and preconcentration of acetaminophen. The effect of important parameters on the extraction ofanalyte was studied and optimized. The extracted acetaminophen was measured by gold-silver nanoparticlefunctionalized with polyethyleneimine as a colorimetric sensor. The linear range was achieved in the range of0.1-20.0 μg L-1 for acetaminophen (R2 = 0.9972) with a limit of detection of 0.029 g L-1. The intra-and inter-dayrelative standard deviations for six measurements at the concentration level of 5.0 μg L-1 acetaminophen werefound to be 2.6 and 4.2 % respectively
پژوهشگران فاطمه محسنی نصرآباد (نفر اول)، علی محمد حاجی شعبانی (نفر دوم)، شایسته دادفرنیا (نفر سوم)، رویا افشاری پور (نفر چهارم)، محمدجواد جهانشاهی (نفر پنجم)