مشخصات پژوهش

صفحه نخست /Synthesis of Triazin ...
عنوان
Synthesis of Triazin Compounds Using Acid Catalyst
نوع پژوهش مقاله ارائه شده
کلیدواژه‌ها
Catalyst, Triazine compound, Phytic acid, Graphitic carbon nitride
چکیده
introduction: Triazine is a six-membered heterocyclic ring containing three nitrogen atoms in which nitrogen replaces the carbon-hydrogen unit in the benzene ring. Based on the position of the nitrogen in the ring system, there are three isomer forms, 1,2,3-triazine, 1,2,4-triazine and 1,3,5-triazine [1]. Methods: Phytic acid doped graphitic carbon nitride was synthesized [2]. For the synthesis of triazin compounds, the solution containing 2-aminobenzamide (0.10 mmol) in distilled water (10 ml) which is stirred with a magnetic stirrer at 0 °C, and then catalyst (15 mg) and n-butyl nitrite. (1.2 mmol) was added to the reaction mixture and stirred for 1.5 hours. The precipitated product was filtered and washed with distilled water. The crude product was purified by recrystallization from ethanol. Results and Discussion: 903 All synthesized compounds were characterized by nuclear magnetic resonance spectroscopy. Based on the results, the prepared catalyst offers a sustainable, environmentally friendly and cost-effective method for the synthesis of triazine compounds (Scheme 1). High yield of products (95%), high speed and simplicity of the method are other advantages of the presented method.
پژوهشگران سبحان یادگاری (نفر اول)، ندا سیدی (نفر دوم)