Bio iron oxide was synthesized from natural Sesbania sesban plant and modified by a molybdenum
complex (Fe2O3/MoSB). Fe2O3/MoSB was deposited on polyvinyl alcohol (PVA) using a conventional
single nozzle electrospinning technique (PVA/Fe2O3/MoSB). TEM, SEM, AFM, FT-IR, TGA, EDAX, and
elemental analysis were used to determine fiber compositional information. The catalytic efficiency of
electrospun PVA/Fe2O3/MoSB nanofiber in the oxidation of alcohols was exploited. The green reactions
were conducted at solvent free conditions as a green media in the presence of H2O2 to have the desired
aldehydes and tert-butyl hydrogen peroxide to obtain acid products in high yields and excellent selectivity.
The survival of this nanocomposite was investigated and it could be reused and recycled in
consecutive runs